Information card for entry 4068967

Structure parameters

• Formula: C16 H38 O4 P4 Ru
• Calculated formula: C16 H38 O4 P4 Ru
• Title of publication: Insertion of CO2into the Ru−C Bonds ofcis-andtrans-Ru(dmpe)2Me2(dmpe = Me2PCH2CH2PMe2)
• Authors of publication: Allen, Olivia R.; Dalgarno, Scott J.; Field, Leslie D.; Jensen, Paul; Willis, Anthony C.
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 8
• Pages of publication: 2385
• a: 9.0425 ± 0.0001 Å
• b: 9.0425 ± 0.0001 Å
• c: 29.079 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2377.7 ± 0.05 ų
• Cell temperature: 200 K
• Ambient diffraction temperature: 200 K
• Number of distinct elements: 5
• Space group number: 96
• Hermann-Mauguin space group symbol: P 43 21 2
• Hall space group symbol: P 4nw 2abw
• Residual factor for all reflections: 0.0186
• Residual factor for significantly intense reflections: 0.0164
• Weighted residual factors for all reflections: 0.0421
• Weighted residual factors for significantly intense reflections: 0.0398
• Weighted residual factors for all reflections included in the refinement: 0.0421
• Goodness-of-fit parameter for all reflections included in the refinement: 0.8941
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No