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Information card for entry 4068984
Preview
Coordinates | 4068984.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C22 H62 B2 O P2 Pb Si4 |
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Calculated formula | C22 H62 B2 O P2 Pb Si4 |
SMILES | [Pb]1[C@]([Si](C)(C)C)([Si](C)(C)CC[Si](C)(C)[C@]1([Si](C)(C)C)[P]([BH3])(C)C)[P]([BH3])(C)C.O(CC)CC.[Pb]1[C@@]([Si](C)(C)C)([Si](C)(C)CC[Si](C)(C)[C@@]1([Si](C)(C)C)[P]([BH3])(C)C)[P]([BH3])(C)C.O(CC)CC |
Title of publication | Seven-Membered Cyclic Dialkylstannylene and -Plumbylene Compounds Stabilized by Agostic-type B−H···E Interactions [E = Sn, Pb] |
Authors of publication | Izod, Keith; Wills, Corinne; Clegg, William; Harrington, Ross W. |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 7 |
Pages of publication | 2211 |
a | 16.168 ± 0.003 Å |
b | 20.182 ± 0.007 Å |
c | 21.656 ± 0.009 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 7066 ± 4 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 7 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0718 |
Residual factor for significantly intense reflections | 0.0302 |
Weighted residual factors for significantly intense reflections | 0.0493 |
Weighted residual factors for all reflections included in the refinement | 0.0623 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.053 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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