Information card for entry 4068986

Structure parameters

• Formula: C39 H68 N3 O2 Si4 Y
• Calculated formula: C39 H68 N3 O2 Si4 Y
• Title of publication: Bis- and Mono(amidate) Complexes of Yttrium: Synthesis, Characterization, and Use as Precatalysts for the Hydroamination of Aminoalkenes
• Authors of publication: Stanlake, Louisa J. E.; Schafer, Laurel L.
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 14
• Pages of publication: 3990
• a: 11.6377 ± 0.0014 Å
• b: 19.076 ± 0.002 Å
• c: 20.423 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4533.9 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0877
• Residual factor for significantly intense reflections: 0.0466
• Weighted residual factors for significantly intense reflections: 0.0787
• Weighted residual factors for all reflections included in the refinement: 0.089
• Goodness-of-fit parameter for all reflections included in the refinement: 0.998
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No