Information card for entry 4069000

Structure parameters

• Formula: C35 H28 N2 O Si
• Calculated formula: C35 H28 N2 O Si
• SMILES: [Si](c1ccccc1)(c1ccccc1)(c1ccccc1)c1cc(C)cc(c1O)/C=N/c1cccc2cccnc12
• Title of publication: Chromium(III) Complexes of Sterically Crowded Bidentante {ONR} and Tridentate {ONNR} Naphthoxy-Imine Ligands: Syntheses, Structures, and Use in Ethylene Oligomerization‡
• Authors of publication: Kirillov, Evgueni; Roisnel, Thierry; Razavi, Abbas; Carpentier, Jean-François
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 8
• Pages of publication: 2401
• a: 10.9845 ± 0.0005 Å
• b: 12.187 ± 0.0006 Å
• c: 20.0955 ± 0.001 Å
• α: 90°
• β: 94.952 ± 0.002°
• γ: 90°
• Cell volume: 2680.1 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0514
• Residual factor for significantly intense reflections: 0.0438
• Weighted residual factors for significantly intense reflections: 0.0996
• Weighted residual factors for all reflections included in the refinement: 0.1054
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No