Crystallography Open Database

Information card for entry 4069050

Preview

Coordinates	4069050.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C31 H52 Os Ru2
Calculated formula	C30.6 H15.8 Os Ru2
Title of publication	Synthesis of Heterometallic Trinuclear Polyhydrido Clusters Containing Ruthenium and Osmium and Their Electronic and Structural Deviation from Homometallic Systems
Authors of publication	Kameo, Hajime; Shima, Takanori; Nakajima, Yumiko; Suzuki, Hiroharu
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	8
Pages of publication	2535
a	11.1842 ± 0.0003 Å
b	19.0686 ± 0.0008 Å
c	29.0602 ± 0.0008 Å
α	90°
β	91.923 ± 0.0008°
γ	90°
Cell volume	6194.1 ± 0.4 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0441
Residual factor for significantly intense reflections	0.0387
Weighted residual factors for significantly intense reflections	0.0964
Weighted residual factors for all reflections included in the refinement	0.0998
Goodness-of-fit parameter for all reflections included in the refinement	1.054
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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