Information card for entry 4069052

Structure parameters

• Formula: C59 H81 B O Os Ru2
• Calculated formula: C58.6 H71.8 B O Os Ru2
• Title of publication: Synthesis of Heterometallic Trinuclear Polyhydrido Clusters Containing Ruthenium and Osmium and Their Electronic and Structural Deviation from Homometallic Systems
• Authors of publication: Kameo, Hajime; Shima, Takanori; Nakajima, Yumiko; Suzuki, Hiroharu
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 8
• Pages of publication: 2535
• a: 10.5832 ± 0.0003 Å
• b: 14.6209 ± 0.0004 Å
• c: 17.4584 ± 0.0006 Å
• α: 86.011 ± 0.001°
• β: 87.972 ± 0.0013°
• γ: 88.627 ± 0.001°
• Cell volume: 2692.58 ± 0.14 ų
• Cell temperature: 183 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0381
• Residual factor for significantly intense reflections: 0.0303
• Weighted residual factors for significantly intense reflections: 0.0733
• Weighted residual factors for all reflections included in the refinement: 0.0768
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No