Information card for entry 4069132

Structure parameters

• Common name: 9b
• Formula: C34 H48 B Cl5 F4 N4 Pd2
• Calculated formula: C34 H48 B Cl5 F4 N4 Pd2
• SMILES: [Pd]12([Cl][Pd]3([n]4[n]2c(C=[N]1c1c(cccc1C(C)C)C(C)C)ccc4C=[N]3c1c(cccc1C(C)C)C(C)C)C)C.ClCCl.ClCCl.[B](F)(F)(F)[F-]
• Title of publication: Synthesis and Characterization of Proximal Dinuclear Complexes of Palladium Supported by 2,6-Bis(arylimino)phenoxy (aryl = 2,6-diisopropylphenyl and 2,4,6-tri-tert-butylphenyl) and 3,6-Bis(imino(2,6-diisopropylphenyl))pyridazine Ligands
• Authors of publication: Ohno, Kouji; Arima, Kenji; Tanaka, Shinji; Yamagata, Tsuneaki; Tsurugi, Hayato; Mashima, Kazushi
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 11
• Pages of publication: 3256
• a: 10.2797 ± 0.0015 Å
• b: 31.117 ± 0.004 Å
• c: 13.3146 ± 0.0018 Å
• α: 90°
• β: 100.966 ± 0.007°
• γ: 90°
• Cell volume: 4181.2 ± 1 ų
• Cell temperature: 114 ± 2 K
• Ambient diffraction temperature: 114 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0858
• Residual factor for significantly intense reflections: 0.061
• Weighted residual factors for significantly intense reflections: 0.1722
• Weighted residual factors for all reflections included in the refinement: 0.1917
• Goodness-of-fit parameter for all reflections included in the refinement: 1.076
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No