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Information card for entry 4069137
Preview
Coordinates | 4069137.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C37 H56 Si2 Zr |
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Calculated formula | C37 H56 Si2 Zr |
SMILES | [Zr]123456789([c]%10([c]%111[c]2(c(c(c(c%11C)C)C)C)[c]13[c]4%10c(c(c(c1C)C)C)C)C)(CC(C)C)[cH]1[c]5([cH]6[cH]7[c]81[Si](C9)(C)C)[Si](C)(C)C |
Title of publication | Octa- and Nonamethylfluorenyl Complexes of Zirconium(IV): Reactive Hydride Derivatives and Reversible Hydrogen Migration between the Metal and the Fluorenyl Ligand |
Authors of publication | Bazinet, Patrick; Tilley, T. Don |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 7 |
Pages of publication | 2285 |
a | 10.9001 ± 0.0017 Å |
b | 11.1535 ± 0.0017 Å |
c | 15.461 ± 0.002 Å |
α | 73.957 ± 0.002° |
β | 87.293 ± 0.002° |
γ | 76.215 ± 0.002° |
Cell volume | 1754.1 ± 0.4 Å3 |
Cell temperature | 152 ± 2 K |
Ambient diffraction temperature | 152 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.087 |
Residual factor for significantly intense reflections | 0.057 |
Weighted residual factors for significantly intense reflections | 0.138 |
Weighted residual factors for all reflections included in the refinement | 0.1503 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.039 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4069137.html
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Users of the data should acknowledge the original authors of the
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