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Information card for entry 4069165
Preview
Coordinates | 4069165.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C41 H66 B F4 N O Os P2 |
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Calculated formula | C41 H66 B F4 N O Os P2 |
SMILES | [Os]1(/C=C/C(=C)C)([P](C(C)C)(C(C)C)C(C)C)([P](C(C)C)(C(C)C)C(C)C)(O[N]1=C(C)C)#CC=C(c1ccccc1)c1ccccc1.[B](F)(F)(F)[F-] |
Title of publication | Selectivity of Allenylidene versus Butadienyl Protonation in an Osmium−Bisphosphine System |
Authors of publication | Bolaño, Tamara; Collado, Alba; Esteruelas, Miguel A.; Oñate, Enrique |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 7 |
Pages of publication | 2107 |
a | 20.801 ± 0.003 Å |
b | 11.0977 ± 0.0016 Å |
c | 20.539 ± 0.003 Å |
α | 90° |
β | 113.895 ± 0.005° |
γ | 90° |
Cell volume | 4334.9 ± 1.1 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 8 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0914 |
Residual factor for significantly intense reflections | 0.0503 |
Weighted residual factors for significantly intense reflections | 0.0923 |
Weighted residual factors for all reflections included in the refinement | 0.1043 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.994 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4069165.html
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Users of the data should acknowledge the original authors of the
structural data.