Information card for entry 4069186

Structure parameters

• Common name: Zirconium bis(trimethylsilyl)amide chloride THF
• Chemical name: Zirconium bis(trimethylsilyl)amide chloride THF
• Formula: C16 H44 Cl2 N2 O Si4 Zr
• Calculated formula: C16 H44 Cl2 N2 O Si4 Zr
• SMILES: C[Si](C)(C)N([Si](C)(C)C)[Zr](Cl)(Cl)(N([Si](C)(C)C)[Si](C)(C)C)[O]1CCCC1
• Title of publication: Synthesis and Characterization of Group 4 Amide Chloride and Amide Imide Complexes
• Authors of publication: Yu, Xianghua; Chen, Shu-Jian; Wang, Xiaoping; Chen, Xue-Tai; Xue, Zi-Ling
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 15
• Pages of publication: 4269
• a: 15.943 ± 0.006 Å
• b: 25.876 ± 0.01 Å
• c: 13.86 ± 0.005 Å
• α: 90°
• β: 93.42 ± 0.007°
• γ: 90°
• Cell volume: 5708 ± 4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0562
• Residual factor for significantly intense reflections: 0.0336
• Weighted residual factors for significantly intense reflections: 0.0896
• Weighted residual factors for all reflections included in the refinement: 0.1197
• Goodness-of-fit parameter for all reflections included in the refinement: 0.738
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No