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Information card for entry 4069223
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Coordinates | 4069223.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | [{Pd(PPh3)}2(SeTrip)2]_2 CH2Cl2 |
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Chemical name | [{Pd(PPh3)}2(SeTrip)2]_2 CH2Cl2 |
Formula | C78 H60 Cl4 P2 Pd2 Se2 |
Calculated formula | C78 H60 Cl4 P2 Pd2 Se2 |
Title of publication | Reactions of 9-Triptyceneselenol with Palladium(0) Complexes: Unexpected Formations of the Dinuclear Palladium(I) Complex [{Pd(PPh3)}2(μ-SeTrip)2] and Five-Membered Selenapalladacycle [Pd(η2(C,Se)-Trip)(dppe)] |
Authors of publication | Nakata, Norio; Uchiumi, Rei; Yoshino, Tomoharu; Ikeda, Takashige; Kamon, Hitomi; Ishii, Akihiko |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 7 |
Pages of publication | 1981 |
a | 11.2728 ± 0.0007 Å |
b | 12.3538 ± 0.0008 Å |
c | 13.3474 ± 0.0009 Å |
α | 67.228 ± 0.001° |
β | 72.261 ± 0.002° |
γ | 89.915 ± 0.001° |
Cell volume | 1617.99 ± 0.18 Å3 |
Cell temperature | 103 ± 2 K |
Ambient diffraction temperature | 103 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0591 |
Residual factor for significantly intense reflections | 0.0465 |
Weighted residual factors for significantly intense reflections | 0.1159 |
Weighted residual factors for all reflections included in the refinement | 0.1241 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.029 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4069223.html
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structural data.