Crystallography Open Database

Information card for entry 4069313

Preview

Coordinates	4069313.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C31.5 H50 N3 O0.5 Th
Calculated formula	C31.5 H50 N3 O0.5 Th
Title of publication	Insertion of Carbodiimides and Organic Azides into Actinide−Carbon Bonds
Authors of publication	Evans, William J.; Walensky, Justin R.; Ziller, Joseph W.; Rheingold, Arnold L.
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	12
Pages of publication	3350
a	9.9109 ± 0.0007 Å
b	10.7104 ± 0.0008 Å
c	14.9504 ± 0.0011 Å
α	85.573 ± 0.001°
β	72.417 ± 0.001°
γ	75.489 ± 0.001°
Cell volume	1464.58 ± 0.19 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0234
Residual factor for significantly intense reflections	0.023
Weighted residual factors for significantly intense reflections	0.0536
Weighted residual factors for all reflections included in the refinement	0.0537
Goodness-of-fit parameter for all reflections included in the refinement	1.219
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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