Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4069378
Preview
Coordinates | 4069378.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | 1,2-Bis{bis[bis(trimethylsilyl)methyl]isopropylsilyl}- 3,5,8-triphenyl-2,6,7-triaza-1,4-disila- bicyclo[2.2.2]oct-2,5,7-triene |
---|---|
Formula | C65.5 H117 N3 Si12 |
Calculated formula | C65.5 H117 N3 Si12 |
Title of publication | Reactivity of the Disilyne RSiSiR (R = SiiPr[CH(SiMe3)2]2) toward Nitriles: Unexpected Formation of Triaza-1,4-disilabicyclo[2.2.2]octa-2,5,7-triene Derivatives |
Authors of publication | Takeuchi, Katsuhiko; Ichinohe, Masaaki; Sekiguchi, Akira; Guo, Jing-Dong; Nagase, Shigeru |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 9 |
Pages of publication | 2658 |
a | 11.937 ± 0.0006 Å |
b | 18.268 ± 0.0009 Å |
c | 20.038 ± 0.0007 Å |
α | 67.498 ± 0.002° |
β | 79.296 ± 0.003° |
γ | 75.67 ± 0.002° |
Cell volume | 3891 ± 0.3 Å3 |
Cell temperature | 150 ± 0.1 K |
Ambient diffraction temperature | 150 ± 0.1 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0847 |
Residual factor for significantly intense reflections | 0.0474 |
Weighted residual factors for significantly intense reflections | 0.1116 |
Weighted residual factors for all reflections included in the refinement | 0.1222 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.888 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4069378.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.