Information card for entry 4069438

Structure parameters

• Formula: C44 H80 N6 O2 Si8 Sm2
• Calculated formula: C44 H80 N6 O2 Si8 Sm2
• Title of publication: Synthesis, Characterization, Selective Catalytic Activity, and Reactivity of Rare Earth Metal Amides with Different Metal−Nitrogen Bonds
• Authors of publication: Zhu, Xiancui; Fan, Jiaxi; Wu, Yunjun; Wang, Shaowu; Zhang, Lijun; Yang, Gaosheng; Wei, Yun; Yin, Chengwei; Zhu, Hong; Wu, Shihong; Zhang, Hongtao
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 13
• Pages of publication: 3882
• a: 11.4255 ± 0.0017 Å
• b: 15.649 ± 0.002 Å
• c: 19.306 ± 0.004 Å
• α: 113.385 ± 0.002°
• β: 95.885 ± 0.002°
• γ: 104.396 ± 0.002°
• Cell volume: 2989.2 ± 0.9 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0621
• Residual factor for significantly intense reflections: 0.0517
• Weighted residual factors for significantly intense reflections: 0.1481
• Weighted residual factors for all reflections included in the refinement: 0.1535
• Goodness-of-fit parameter for all reflections included in the refinement: 1.103
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No