Information card for entry 4069558

Structure parameters

• Common name: 9c
• Chemical name: Chlorodimethyl[N-(benzylideneimino)acetamidomethyl]silane
• Formula: C12 H15 Cl N2 O Si
• Calculated formula: C12 H15 Cl N2 O Si
• Title of publication: Regioselective Intramolecular Chloride Displacement Leading to Five- or Six-Membered Chelate-Ring Closure and Pentacoordinate Silicon Complexes: A Facile Wawzonek Rearrangement†
• Authors of publication: Yakubovich, Shiri; Gostevskii, Boris; Kalikhman, Inna; Kost, Daniel
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 14
• Pages of publication: 4126
• a: 19.307 ± 0.005 Å
• b: 6.9388 ± 0.0017 Å
• c: 10.358 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1387.6 ± 0.6 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0448
• Residual factor for significantly intense reflections: 0.037
• Weighted residual factors for significantly intense reflections: 0.0851
• Weighted residual factors for all reflections included in the refinement: 0.0896
• Goodness-of-fit parameter for all reflections included in the refinement: 0.961
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No