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Information card for entry 4069569
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Coordinates | 4069569.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | compound4d |
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Formula | C57 H87 N2 P2 Si7 |
Calculated formula | C57 H87 N2 P2 Si7 |
Title of publication | [4+2] Cycloaddition of 9-Anthryldiphosphene with Electron-Deficient Olefins: Transformation of a Diaryldiphosphene to Alkylaryldiphosphenes |
Authors of publication | Tsurusaki, Akihiro; Sasamori, Takahiro; Tokitoh, Norihiro |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 13 |
Pages of publication | 3604 |
a | 11.804 ± 0.005 Å |
b | 12.676 ± 0.006 Å |
c | 22.115 ± 0.009 Å |
α | 74.025 ± 0.011° |
β | 79.207 ± 0.011° |
γ | 88.701 ± 0.011° |
Cell volume | 3123 ± 2 Å3 |
Cell temperature | 103 ± 2 K |
Ambient diffraction temperature | 103 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1348 |
Residual factor for significantly intense reflections | 0.0747 |
Weighted residual factors for significantly intense reflections | 0.1225 |
Weighted residual factors for all reflections included in the refinement | 0.1504 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.113 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4069569.html
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