Information card for entry 4069575

Structure parameters

• Formula: C27 H69 K O6 Si7
• Calculated formula: C27 H69 K O6 Si7
• SMILES: [K]12345([O]6CC[O]1CC[O]2CC[O]3CC[O]4CC[O]5CC6)[Si]([Si]([Si](C)(C)C)(C)C)([Si]([Si](C)(C)C)(C)C)[Si]([Si](C)(C)C)(C)C
• Title of publication: Multiple Silyl Exchange Reactions: A Way to Spirooligosilanes
• Authors of publication: Hlina, Johann; Mechtler, Christian; Wagner, Harald; Baumgartner, Judith; Marschner, Christoph
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 14
• Pages of publication: 4065
• a: 12.684 ± 0.003 Å
• b: 18.764 ± 0.004 Å
• c: 19.958 ± 0.004 Å
• α: 90°
• β: 97.66 ± 0.03°
• γ: 90°
• Cell volume: 4707.7 ± 1.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1956
• Residual factor for significantly intense reflections: 0.0911
• Weighted residual factors for significantly intense reflections: 0.2164
• Weighted residual factors for all reflections included in the refinement: 0.2695
• Goodness-of-fit parameter for all reflections included in the refinement: 0.927
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No