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Information card for entry 4069643
Preview
Coordinates | 4069643.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C23 H51 N Os P2 |
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Calculated formula | C23 H51 N Os P2 |
SMILES | [OsH4]([P](C(C)C)(C(C)C)C(C)C)([P](C(C)C)(C(C)C)C(C)C)[n]1ccccc1 |
Title of publication | Stoichiometric and Catalytic Deuteration of Pyridine and Methylpyridines by H/D Exchange with Benzene-d6Promoted by an Unsaturated Osmium Tetrahydride Species |
Authors of publication | Eguillor, Beatriz; Esteruelas, Miguel A.; García-Raboso, Jorge; Oliván, Montserrat; Oñate, Enrique |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 13 |
Pages of publication | 3700 |
a | 7.9417 ± 0.0014 Å |
b | 18.47 ± 0.003 Å |
c | 18.331 ± 0.003 Å |
α | 90° |
β | 93.388 ± 0.003° |
γ | 90° |
Cell volume | 2684.2 ± 0.8 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0958 |
Residual factor for significantly intense reflections | 0.0462 |
Weighted residual factors for significantly intense reflections | 0.0725 |
Weighted residual factors for all reflections included in the refinement | 0.0811 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.746 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4069643.html
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