Information card for entry 4069653
| Formula |
C32 H34 O4 Ru2 |
| Calculated formula |
C32 H34 O4 Ru2 |
| Title of publication |
Reactions of Dihydrooctamethyl-s-indacene and 1,2,3,4,7-Pentamethylindene with Ru3(CO)12: Intramolecular sp3C−H Activation |
| Authors of publication |
Xu, Kun; Li, Bin; Xu, Shansheng; Song, Haibin; Wang, Baiquan |
| Journal of publication |
Organometallics |
| Year of publication |
2009 |
| Journal volume |
28 |
| Journal issue |
15 |
| Pages of publication |
4438 |
| a |
9.4669 ± 0.0019 Å |
| b |
9.845 ± 0.002 Å |
| c |
15.165 ± 0.003 Å |
| α |
104.11 ± 0.03° |
| β |
91 ± 0.03° |
| γ |
91.54 ± 0.03° |
| Cell volume |
1369.8 ± 0.5 Å3 |
| Cell temperature |
113 ± 2 K |
| Ambient diffraction temperature |
113 ± 2 K |
| Number of distinct elements |
4 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0804 |
| Residual factor for significantly intense reflections |
0.0675 |
| Weighted residual factors for significantly intense reflections |
0.1687 |
| Weighted residual factors for all reflections included in the refinement |
0.1727 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.048 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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https://www.crystallography.net/4069653.html
