Information card for entry 4069728

Structure parameters

• Formula: C121 H82 B2 Cl2 F40 Ir2 N4 Si2
• Calculated formula: C121 H82 B2 Cl2 F40 Ir2 N4 Si2
• Title of publication: Synthesis and Reactivity of Iridium and Rhodium Silyl Complexes Supported by a Bipyridine Ligand
• Authors of publication: McBee, Jennifer L.; Tilley, T. Don
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 17
• Pages of publication: 5072
• a: 10.357 ± 0.002 Å
• b: 20.25 ± 0.004 Å
• c: 27.327 ± 0.006 Å
• α: 83.719 ± 0.003°
• β: 82.617 ± 0.003°
• γ: 88.458 ± 0.003°
• Cell volume: 5649 ± 2 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0601
• Residual factor for significantly intense reflections: 0.037
• Weighted residual factors for significantly intense reflections: 0.0734
• Weighted residual factors for all reflections included in the refinement: 0.0792
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No