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Information card for entry 4069788
Preview
Coordinates | 4069788.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C36 H61 N3 O2 Si4 Yb2 |
---|---|
Calculated formula | C36 H61 N3 O2 Si4 Yb2 |
SMILES | [Yb]123456789%10%11[N]%12([Yb]%13%14%15%16(N([Si](C)(C)C)[Si](C)(C)C)([O]1c1n([Si]([c]%173[c]4([c]5([c]6([c]7%17C)C)C)C)(C)C)ccc1)[c]1([Si](O2)(C)C)[c]%13([c]%14([c]%15([c]%161C)C)C)C)[CH]8=[CH]9[CH]%10=[CH]%11%12 |
Title of publication | C−H and Si−N Bond Oxygenations of a Divalent Ytterbium Amide of the Pyrrolyl-Cyclopentadienyl Ligand |
Authors of publication | Hao, Jingjun; Song, Haibin; Cui, Chunming |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 14 |
Pages of publication | 3970 |
a | 12.099 ± 0.002 Å |
b | 26.325 ± 0.005 Å |
c | 13.147 ± 0.003 Å |
α | 90° |
β | 98.66 ± 0.03° |
γ | 90° |
Cell volume | 4139.7 ± 1.4 Å3 |
Cell temperature | 113 ± 2 K |
Ambient diffraction temperature | 113 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0625 |
Residual factor for significantly intense reflections | 0.047 |
Weighted residual factors for significantly intense reflections | 0.1001 |
Weighted residual factors for all reflections included in the refinement | 0.1055 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.021 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4069788.html
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Users of the data should acknowledge the original authors of the
structural data.