Information card for entry 4069797

Structure parameters

• Formula: C94 H81 Ag4 F24 N19 P4
• Calculated formula: C94 H81 Ag4 F24 N19 P4
• Title of publication: New Pincer CC′C Complexes of Nickel(II) via Chloronickelation of Alkyne-Bearing N-Heterocyclic Carbenes
• Authors of publication: Liu, Ailing; Zhang, Xiaoming; Chen, Wanzhi
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 16
• Pages of publication: 4868
• a: 14.6118 ± 0.0015 Å
• b: 22.666 ± 0.002 Å
• c: 15.5491 ± 0.0017 Å
• α: 90°
• β: 100.227 ± 0.002°
• γ: 90°
• Cell volume: 5067.9 ± 0.9 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 7
• Hermann-Mauguin space group symbol: P 1 n 1
• Hall space group symbol: P -2yac
• Residual factor for all reflections: 0.106
• Residual factor for significantly intense reflections: 0.0569
• Weighted residual factors for significantly intense reflections: 0.1354
• Weighted residual factors for all reflections included in the refinement: 0.1705
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No