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Information card for entry 4069815
Preview
Coordinates | 4069815.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C52 H48 Cl2 P2 Pd2 |
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Calculated formula | C52 H48 Cl2 P2 Pd2 |
SMILES | c12ccc(C)cc2cc(C)c2c1[Pd]1([Cl][Pd]3(c4c5ccc(C)cc5cc(C)c4[C@@H]([P]3(c3ccccc3)c3ccccc3)C)[Cl]1)[P](c1ccccc1)([C@H]2C)c1ccccc1 |
Title of publication | Synthesis, Coordination Characteristics, Conformational Behavior, and Bond Reactivity Studies of a Novel Chiral Phosphapalladacycle Complex |
Authors of publication | Ding, Yi; Chiang, Minyi; Pullarkat, Sumod A.; Li, Yongxin; Leung, Pak-Hing |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 15 |
Pages of publication | 4358 |
a | 21.9239 ± 0.001 Å |
b | 6.8683 ± 0.0003 Å |
c | 15.0574 ± 0.0007 Å |
α | 90° |
β | 94.667 ± 0.002° |
γ | 90° |
Cell volume | 2259.82 ± 0.18 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 5 |
Space group number | 5 |
Hermann-Mauguin space group symbol | C 1 2 1 |
Hall space group symbol | C 2y |
Residual factor for all reflections | 0.0633 |
Residual factor for significantly intense reflections | 0.05 |
Weighted residual factors for significantly intense reflections | 0.1393 |
Weighted residual factors for all reflections included in the refinement | 0.1575 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.067 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4069815.html
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