Information card for entry 4069817

Structure parameters

• Formula: C26 H37 Cl4 N3 O3 Pd S
• Calculated formula: C26 H37 Cl4 N3 O3 Pd S
• Title of publication: Synthesis of N-Heterocyclic Carbene-Sulfonate Palladium Complexes
• Authors of publication: Nagai, Yusuke; Kochi, Takuya; Nozaki, Kyoko
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 20
• Pages of publication: 6131
• a: 13.175 ± 0.007 Å
• b: 13.756 ± 0.007 Å
• c: 19.151 ± 0.01 Å
• α: 90.949 ± 0.008°
• β: 100.141 ± 0.008°
• γ: 97.566 ± 0.008°
• Cell volume: 3384 ± 3 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0937
• Residual factor for significantly intense reflections: 0.0835
• Weighted residual factors for significantly intense reflections: 0.1891
• Weighted residual factors for all reflections included in the refinement: 0.1948
• Goodness-of-fit parameter for all reflections included in the refinement: 1.145
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No