Information card for entry 4069842

Structure parameters

• Formula: C12 H19 Cl I O5 P Si2 W
• Calculated formula: C12 H19 Cl I O5 P Si2 W
• SMILES: [W]([P](I)(Cl)C([Si](C)(C)C)[Si](C)(C)C)(C#[O])(C#[O])(C#[O])(C#[O])C#[O]
• Title of publication: Investigations on the Reactivity of Li/Cl Phosphinidenoid Tungsten Complexes toward Various Iodine Compounds
• Authors of publication: Streubel, Rainer; Özbolat-Schön, Aysel; Bode, Maren; Daniels, Jörg; Schnakenburg, Gregor; Teixidor, Francesc; Vinas, Clara; Vaca, Albert; Pepiol, Ariadna; Farràs, Pau
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 20
• Pages of publication: 6031
• a: 14.7403 ± 0.0004 Å
• b: 9.6381 ± 0.0002 Å
• c: 15.323 ± 0.0003 Å
• α: 90°
• β: 101.397 ± 0.001°
• γ: 90°
• Cell volume: 2133.99 ± 0.08 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0448
• Residual factor for significantly intense reflections: 0.0394
• Weighted residual factors for significantly intense reflections: 0.1017
• Weighted residual factors for all reflections included in the refinement: 0.1042
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No