Information card for entry 4069844

Structure parameters

• Formula: C37 H60 N4 Si2
• Calculated formula: C37 H60 N4 Si2
• SMILES: [Si]1(N(c2c(cccc2C(C)C)C(C)C)[Si](N1c1c(cccc1C(C)C)C(C)C)(C)C)c1[n+](cn(c1)C(C)(C)C)C(C)(C)C
• Title of publication: Dehydrochlorination to Silylenes by N-Heterocyclic Carbenes
• Authors of publication: Cui, Haiyan; Shao, Yanjun; Li, Xiaofei; Kong, Lingbing; Cui, Chunming
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 17
• Pages of publication: 5191
• a: 29.013 ± 0.006 Å
• b: 11.349 ± 0.002 Å
• c: 23.425 ± 0.005 Å
• α: 90°
• β: 99.15 ± 0.03°
• γ: 90°
• Cell volume: 7615 ± 3 ų
• Cell temperature: 113 ± 2 K
• Ambient diffraction temperature: 113 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0709
• Residual factor for significantly intense reflections: 0.0549
• Weighted residual factors for significantly intense reflections: 0.1352
• Weighted residual factors for all reflections included in the refinement: 0.146
• Goodness-of-fit parameter for all reflections included in the refinement: 1.089
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No