Crystallography Open Database

Information card for entry 4069857

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Coordinates	4069857.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C39 H58 N O Si2 Y
Calculated formula	C39 H50 N O Si2 Y
Title of publication	Lanthanide Terminal Hydride Complexes Bearing Two Sterically Demanding C5Me4SiMe3Ligands. Synthesis, Structure, and Reactivity
Authors of publication	Takenaka, Yasumasa; Hou, Zhaomin
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	17
Pages of publication	5196
a	11.497 ± 0.0007 Å
b	13.5554 ± 0.0008 Å
c	14.0902 ± 0.0009 Å
α	105.826 ± 0.001°
β	100.449 ± 0.001°
γ	108.506 ± 0.001°
Cell volume	1915.1 ± 0.2 Å³
Cell temperature	173 ± 1 K
Ambient diffraction temperature	173 ± 1 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0724
Residual factor for significantly intense reflections	0.0502
Weighted residual factors for significantly intense reflections	0.1168
Weighted residual factors for all reflections included in the refinement	0.1198
Goodness-of-fit parameter for all reflections included in the refinement	1.36
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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