Information card for entry 4069859

Structure parameters

• Formula: C34 H60 Dy Ir Si2
• Calculated formula: C34 H60 Dy Ir Si2
• SMILES: [Ir]123456([H][Dy]789%10%11%12%13%14([c]%15([Si](C)(C)C)[c]8([c]9([c]%10([c]%11%15C)C)C)C)([c]8([Si](C)(C)C)[c]%12([c]%13([c]%14([c]78C)C)C)C)([H]5)[H]6)[c]5([c]4([c]3([c]2([c]15C)C)C)C)C
• Title of publication: Lanthanide Terminal Hydride Complexes Bearing Two Sterically Demanding C5Me4SiMe3Ligands. Synthesis, Structure, and Reactivity
• Authors of publication: Takenaka, Yasumasa; Hou, Zhaomin
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 17
• Pages of publication: 5196
• a: 9.915 ± 0.002 Å
• b: 10.976 ± 0.003 Å
• c: 18.149 ± 0.004 Å
• α: 85.138 ± 0.004°
• β: 79.193 ± 0.004°
• γ: 68.926 ± 0.004°
• Cell volume: 1810 ± 0.7 ų
• Cell temperature: 173 ± 1 K
• Ambient diffraction temperature: 173 ± 1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0458
• Residual factor for significantly intense reflections: 0.0383
• Weighted residual factors for significantly intense reflections: 0.0915
• Weighted residual factors for all reflections included in the refinement: 0.0943
• Goodness-of-fit parameter for all reflections included in the refinement: 0.985
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No