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Information card for entry 4069866
Preview
Coordinates | 4069866.cif |
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Original paper (by DOI) | HTML |
Chemical name | (Z)-triethylsilylvinyl mono-nitrosyl bis-tricyclohexylphosphine rhenium bromide |
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Formula | C44 H83 Br N O P2 Re Si |
Calculated formula | C44 H83 Br N O P2 Re Si |
Title of publication | From Alkynes to Carbenes Mediated by [Re(Br)(H)(NO)(PR3)2] (R = Cy,iPr) Complexes |
Authors of publication | Jiang, Yanfeng; Blacque, Olivier; Fox, Thomas; Frech, Christian M.; Berke, Heinz |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 16 |
Pages of publication | 4670 |
a | 12.7359 ± 0.0001 Å |
b | 12.8512 ± 0.0002 Å |
c | 16.2393 ± 0.0002 Å |
α | 69.673 ± 0.001° |
β | 88.298 ± 0.001° |
γ | 70.411 ± 0.001° |
Cell volume | 2336.78 ± 0.06 Å3 |
Cell temperature | 183 ± 2 K |
Ambient diffraction temperature | 183 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0382 |
Residual factor for significantly intense reflections | 0.0294 |
Weighted residual factors for significantly intense reflections | 0.0766 |
Weighted residual factors for all reflections included in the refinement | 0.0782 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.042 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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