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Information card for entry 4069894
Preview
Coordinates | 4069894.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C33 H29 O2.5 P2 |
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Calculated formula | C33 H28 O2.5 P2 |
Title of publication | Synthesis of Biaryl Diphosphines via a Stepwise Regioselective Double Diels−Alder Cycloaddition−Elimination Sequence: Efficient Ligands for the Palladium-Catalyzed Amination of Aromatic Bromides |
Authors of publication | Doherty, Simon; Smyth, Catherine H.; Harrington, Ross W.; Clegg, William |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 17 |
Pages of publication | 5273 |
a | 11.01 ± 0.002 Å |
b | 16.589 ± 0.006 Å |
c | 15.323 ± 0.005 Å |
α | 90° |
β | 101.362 ± 0.016° |
γ | 90° |
Cell volume | 2743.8 ± 1.4 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0634 |
Residual factor for significantly intense reflections | 0.0392 |
Weighted residual factors for significantly intense reflections | 0.0857 |
Weighted residual factors for all reflections included in the refinement | 0.098 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.058 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4069894.html
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