Crystallography Open Database

Information card for entry 4069902

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Coordinates	4069902.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C42.3 H71.92 N2 P Rh
Calculated formula	C42.3 H72.58 N2 P Rh
Title of publication	N-Heterocyclic Carbene Functionalized Group 7−9 Transition Metal Phosphinidene Complexes
Authors of publication	Aktas, Halil; Slootweg, J. Chris; Ehlers, Andreas W.; Lutz, Martin; Spek, Anthony L.; Lammertsma, Koop
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	17
Pages of publication	5166
a	10.4727 ± 0.0003 Å
b	15.1067 ± 0.0004 Å
c	13.7281 ± 0.0002 Å
α	90°
β	95.432 ± 0.002°
γ	90°
Cell volume	2162.14 ± 0.09 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.0351
Residual factor for significantly intense reflections	0.0285
Weighted residual factors for significantly intense reflections	0.0861
Weighted residual factors for all reflections included in the refinement	0.0906
Goodness-of-fit parameter for all reflections included in the refinement	1.053
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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