Information card for entry 4069923

Structure parameters

• Formula: C42 H46 Ge3 P2 Pt
• Calculated formula: C42 H46 Ge3 P2 Pt
• SMILES: [Pt]12([Ge]([Ge]([Ge]1(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)[P](C)(C)CC[P]2(C)C
• Title of publication: Formation and Ring Expansion of Germaplatinacycles via Dehydrogenative Ge−Ge and Ge−Pt Bond-Forming Reactions
• Authors of publication: Tanabe, Makoto; Hanzawa, Masaya; Ishikawa, Naoko; Osakada, Kohtaro
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 20
• Pages of publication: 6014
• a: 17.783 ± 0.007 Å
• b: 15.928 ± 0.008 Å
• c: 15.164 ± 0.005 Å
• α: 90°
• β: 102.04 ± 0.03°
• γ: 90°
• Cell volume: 4201 ± 3 ų
• Cell temperature: 298.1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1378
• Residual factor for significantly intense reflections: 0.0443
• Weighted residual factors for significantly intense reflections: 0.1097
• Weighted residual factors for all reflections included in the refinement: 0.1416
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No