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Information card for entry 4069935
Preview
Coordinates | 4069935.cif |
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Original paper (by DOI) | HTML |
Chemical name | 2,4,6-Tri-tert-butylpyridinium tris(pentafluorophenyl)hydroborate |
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Formula | C38 H38 B F15 N |
Calculated formula | C38 H38 B F15 N |
Title of publication | Metal-Free Hydrogen Activation by the Frustrated Lewis Pairs of ClB(C6F5)2and HB(C6F5)2and Bulky Lewis Bases |
Authors of publication | Jiang, Chunfang; Blacque, Olivier; Berke, Heinz |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 17 |
Pages of publication | 5233 |
a | 9.8216 ± 0.0003 Å |
b | 10.7921 ± 0.0003 Å |
c | 18.7474 ± 0.0006 Å |
α | 74.768 ± 0.003° |
β | 77.215 ± 0.003° |
γ | 78.314 ± 0.003° |
Cell volume | 1847.65 ± 0.1 Å3 |
Cell temperature | 183 ± 2 K |
Ambient diffraction temperature | 183 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1163 |
Residual factor for significantly intense reflections | 0.0495 |
Weighted residual factors for significantly intense reflections | 0.1148 |
Weighted residual factors for all reflections included in the refinement | 0.1364 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.864 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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