Information card for entry 4069937

Structure parameters

• Formula: C53 H86 Si2 Sm2
• Calculated formula: C53 H78 Si2 Sm2
• Title of publication: Anti-Bimetallic Complexes of Divalent Lanthanides with Silylated Pentalene and Cyclooctatetraenyl Bridging Ligands as Molecular Models for Lanthanide-Based Polymers
• Authors of publication: Summerscales, Owen T.; Jones, Simon C.; Cloke, F. Geoffrey N.; Hitchcock, Peter B.
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 20
• Pages of publication: 5896
• a: 7.824 ± 0.0002 Å
• b: 17.3596 ± 0.0005 Å
• c: 18.6606 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2534.51 ± 0.11 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 59
• Hermann-Mauguin space group symbol: P n m m :2
• Hall space group symbol: -P 2c 2bc
• Residual factor for all reflections: 0.0471
• Residual factor for significantly intense reflections: 0.0341
• Weighted residual factors for significantly intense reflections: 0.0853
• Weighted residual factors for all reflections included in the refinement: 0.0916
• Goodness-of-fit parameter for all reflections included in the refinement: 1.074
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No