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Information card for entry 4070004
Preview
Coordinates | 4070004.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C37 H44 F6 N3 P Pd |
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Calculated formula | C37 H44 F6 N3 P Pd |
Title of publication | Rigid, Sterically Diverse N-Heterocyclic Carbene-Pyridine Chelates: Synthesis, Mild Palladation, and Palladium-Catalyzed Allylic Substitution |
Authors of publication | Chianese, Anthony R.; Bremer, Paul T.; Wong, Christina; Reynes, Rae Julienne |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 17 |
Pages of publication | 5244 |
a | 9.12141 ± 0.00015 Å |
b | 13.1251 ± 0.0003 Å |
c | 15.8828 ± 0.0005 Å |
α | 77.754 ± 0.003° |
β | 77.355 ± 0.002° |
γ | 74.5178 ± 0.0019° |
Cell volume | 1764 ± 0.08 Å3 |
Cell temperature | 110 K |
Ambient diffraction temperature | 110 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0385 |
Residual factor for significantly intense reflections | 0.0299 |
Weighted residual factors for all reflections | 0.0746 |
Weighted residual factors for significantly intense reflections | 0.0729 |
Weighted residual factors for all reflections included in the refinement | 0.0746 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.0012 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4070004.html
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