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Information card for entry 4070017
Preview
Coordinates | 4070017.cif |
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Original paper (by DOI) | HTML |
Formula | C19 H17 Cl5 N Na Pd2 Se2 |
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Calculated formula | C19 H17 Cl5 N Na Pd2 Se2 |
SMILES | c1ccccc1[Se]1Cc2cccc(C[Se]3c4ccccc4)[n]2[Pd]13Cl.Cl[Pd](Cl)([Cl-])[Cl-].[Na+] |
Title of publication | Palladium(II) Complexes of the First Pincer (Se,N,Se) Ligand, 2,6-Bis((phenylseleno)methyl)pyridine (L): Solvent-Dependent Formation of [PdCl(L)]Cl and Na[PdCl(L)][PdCl4] and High Catalytic Activity for the Heck Reaction |
Authors of publication | Das, Dipanwita; Rao, G. K.; Singh, Ajai K. |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 20 |
Pages of publication | 6054 |
a | 8.792 ± 0.003 Å |
b | 12.411 ± 0.004 Å |
c | 12.624 ± 0.004 Å |
α | 76.084 ± 0.006° |
β | 84.604 ± 0.006° |
γ | 82.053 ± 0.006° |
Cell volume | 1321.6 ± 0.7 Å3 |
Cell temperature | 273 ± 2 K |
Ambient diffraction temperature | 273 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0636 |
Residual factor for significantly intense reflections | 0.059 |
Weighted residual factors for significantly intense reflections | 0.1815 |
Weighted residual factors for all reflections included in the refinement | 0.1857 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.08 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4070017.html
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