Information card for entry 4070025

Structure parameters

• Formula: C48 H40 Cl4 F3 N O3 P2 Ru
• Calculated formula: C48 H39 Cl4 F3 N O3 P2 Ru
• Title of publication: Protonation of a Ruthenium Vinylidene Complex with a NO Ligand Leading to Ruthenium Vinyl Complexes
• Authors of publication: Arikawa, Yasuhiro; Yamasaki, Hayato; Yamaguchi, Mamoru; Umakoshi, Keisuke; Onishi, Masayoshi
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 18
• Pages of publication: 5587
• a: 18.342 ± 0.003 Å
• b: 10.9759 ± 0.0017 Å
• c: 24.148 ± 0.004 Å
• α: 90°
• β: 105.995 ± 0.0004°
• γ: 90°
• Cell volume: 4673.3 ± 1.3 ų
• Cell temperature: 296.1 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0559
• Weighted residual factors for all reflections included in the refinement: 0.1823
• Goodness-of-fit parameter for all reflections included in the refinement: 1.004
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No