Information card for entry 4070040

Structure parameters

• Formula: C36 H46 Fe Ge N2 O2
• Calculated formula: C36 H46 Fe Ge N2 O2
• Title of publication: Isolable Metallo-Germylene and Metallo-Stannylene σ-Complexes with Iron
• Authors of publication: Inoue, Shigeyoshi; Driess, Matthias
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 17
• Pages of publication: 5032
• a: 9.0894 ± 0.0002 Å
• b: 21.8257 ± 0.0005 Å
• c: 17.4797 ± 0.0004 Å
• α: 90°
• β: 102.984 ± 0.002°
• γ: 90°
• Cell volume: 3379.01 ± 0.14 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1285
• Residual factor for significantly intense reflections: 0.0825
• Weighted residual factors for significantly intense reflections: 0.1384
• Weighted residual factors for all reflections included in the refinement: 0.1537
• Goodness-of-fit parameter for all reflections included in the refinement: 1.168
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No