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Information card for entry 4070183
Preview
Coordinates | 4070183.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C34 H43 N5 Ti |
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Calculated formula | C34 H43 N5 Ti |
SMILES | C1CCC2=[N]1[Ti]1345([c]6([c]3([c]5([c]4([c]16C)C)C)C)C)(N2c1cc(cc(c1)C)C)(=NN(C)c1ccccc1)[n]1ccccc1 |
Title of publication | Titanium Hydrazinediido Half-Sandwich Complexes: Highly Active Catalysts for the Hydrohydrazination of Terminal Alkynes at Ambient Temperature |
Authors of publication | Weitershaus, Katharina; Wadepohl, Hubert; Gade, Lutz H. |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 16 |
Pages of publication | 4898 |
a | 11.483 ± 0.002 Å |
b | 17.855 ± 0.003 Å |
c | 15.233 ± 0.003 Å |
α | 90° |
β | 92.644 ± 0.004° |
γ | 90° |
Cell volume | 3119.9 ± 1 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.1073 |
Residual factor for significantly intense reflections | 0.0484 |
Weighted residual factors for significantly intense reflections | 0.1078 |
Weighted residual factors for all reflections included in the refinement | 0.1444 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.069 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4070183.html
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