Information card for entry 4070200

Structure parameters

• Formula: C48 H60 Cr N4 O0.5 P4 W
• Calculated formula: C48 H56 Cr N4 O0.5 P4 W
• Title of publication: Preparation and Protonation of Tungsten- and Molybdenum-Dinitrogen Complexes Bearing Bis(dialkylphosphinobenzene)chromiums as Auxiliary Ligands
• Authors of publication: Yuki, Masahiro; Miyake, Yoshihiro; Nishibayashi, Yoshiaki
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 19
• Pages of publication: 5821
• a: 11.0977 ± 0.0003 Å
• b: 19.5256 ± 0.0006 Å
• c: 21.234 ± 0.0005 Å
• α: 90°
• β: 97.8723 ± 0.0007°
• γ: 90°
• Cell volume: 4557.8 ± 0.2 ų
• Cell temperature: 173.1 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.0435
• Weighted residual factors for all reflections included in the refinement: 0.0567
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No