Information card for entry 4070302

Structure parameters

• Formula: C67 H73 Cl2 N3 O2 Ta
• Calculated formula: C67 H73 Cl2 N3 O2 Ta
• Title of publication: Reactivity of Diazoalkanes with Tantalum(V) Complexes of a Tridentate Amido-Bis(phenolate) Ligand
• Authors of publication: Zarkesh, Ryan A.; Heyduk, Alan F.
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 23
• Pages of publication: 6629
• a: 20.9828 ± 0.0011 Å
• b: 21.2413 ± 0.0011 Å
• c: 15.398 ± 0.0008 Å
• α: 90°
• β: 117.427 ± 0.002°
• γ: 90°
• Cell volume: 6091.5 ± 0.6 ų
• Cell temperature: 143 ± 2 K
• Ambient diffraction temperature: 143 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0508
• Residual factor for significantly intense reflections: 0.0405
• Weighted residual factors for significantly intense reflections: 0.108
• Weighted residual factors for all reflections included in the refinement: 0.1147
• Goodness-of-fit parameter for all reflections included in the refinement: 1.137
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No