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Information card for entry 4070339
Preview
Coordinates | 4070339.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C64 H70 Lu N3 O P2 Si |
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Calculated formula | C64 H70 Lu N3 O P2 Si |
SMILES | c12cc(cc3c4cc(cc5c4n(c13)[Lu]1(c3c(cccc3)P5(c3ccccc3)=[N]1c1ccc(cc1)C(C)C)(C[Si](C)(C)C)([N](c1ccc(cc1)C(C)C)=P2(c1ccccc1)c1ccccc1)[O]1CCCC1)C)C |
Title of publication | Synthesis and Reactivity of Dialkyl Lutetium Complexes Supported by a Novel Bis(phosphinimine)carbazole Pincer Ligand |
Authors of publication | Johnson, Kevin R. D.; Hayes, Paul G. |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 21 |
Pages of publication | 6352 |
a | 10.768 ± 0.0013 Å |
b | 21.278 ± 0.003 Å |
c | 26.917 ± 0.003 Å |
α | 90° |
β | 99.461 ± 0.002° |
γ | 90° |
Cell volume | 6083.4 ± 1.3 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.1316 |
Residual factor for significantly intense reflections | 0.0994 |
Weighted residual factors for significantly intense reflections | 0.2487 |
Weighted residual factors for all reflections included in the refinement | 0.2665 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.06 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4070339.html
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