Crystallography Open Database

Information card for entry 4070347

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Coordinates	4070347.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H60 Al B N6 Yb
Calculated formula	C32 H60 Al B N6 Yb
Title of publication	Monomeric Tetraalkylaluminates of Divalent Ytterbium Stabilized by a Bulky Tris(pyrazolyl)borate Ligand
Authors of publication	Litlabø, Rannveig; Saliu, Kuburat; Ferguson, Michael J.; McDonald, Robert; Takats, Josef; Anwander, Reiner
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	23
Pages of publication	6750
a	12.2403 ± 0.0005 Å
b	12.5915 ± 0.0005 Å
c	13.779 ± 0.0006 Å
α	81.9634 ± 0.0005°
β	81.2313 ± 0.0004°
γ	64.3889 ± 0.0004°
Cell volume	1886.12 ± 0.14 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0188
Residual factor for significantly intense reflections	0.0175
Weighted residual factors for significantly intense reflections	0.0464
Weighted residual factors for all reflections included in the refinement	0.0472
Goodness-of-fit parameter for all reflections included in the refinement	1.036
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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