Synthesis, Structure, and Reactivity of Alkyl-Substituted Half-Sandwich η5-Pentadienyl Complexes of Cobalt
Authors of publication
Ylijoki, Kai E. O.; Witherell, Ross D.; Kirk, Andrew D.; Böcklein, Sebastian; Lofstrand, Verner A.; McDonald, Robert; Ferguson, Michael J.; Stryker, Jeffrey M.
Journal of publication
Organometallics
Year of publication
2009
Journal volume
28
Journal issue
23
Pages of publication
6807
a
6.9631 ± 0.0008 Å
b
13.4708 ± 0.0016 Å
c
16.896 ± 0.002 Å
α
90°
β
99.31 ± 0.002°
γ
90°
Cell volume
1563.9 ± 0.3 Å3
Cell temperature
193 ± 2 K
Ambient diffraction temperature
193 ± 2 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0666
Residual factor for significantly intense reflections
0.0524
Weighted residual factors for significantly intense reflections
0.1372
Weighted residual factors for all reflections included in the refinement
0.1422
Goodness-of-fit parameter for all reflections included in the refinement
