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Information card for entry 4070400
Preview
Coordinates | 4070400.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C30 H45 Cl2 N2 Ni P |
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Calculated formula | C30 H45 Cl2 N2 Ni P |
SMILES | [Ni]([P](C)(C)C)(=C1N(c2c(cccc2C(C)C)C(C)C)C=CN1c1c(C(C)C)cccc1C(C)C)(Cl)Cl |
Title of publication | Group-Transfer Reactions of Ni(II)−Ni(II) Bridging Imido Complexes. Catalytic Formation of Carbodiimides and Isocyanates via Nitrene Transfer from Organoazides |
Authors of publication | Laskowski, Carl A.; Hillhouse, Gregory L. |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 20 |
Pages of publication | 6114 |
a | 14.3647 ± 0.0016 Å |
b | 20.944 ± 0.002 Å |
c | 21.453 ± 0.002 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 6454.2 ± 1.1 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0688 |
Residual factor for significantly intense reflections | 0.0514 |
Weighted residual factors for significantly intense reflections | 0.1326 |
Weighted residual factors for all reflections included in the refinement | 0.1385 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.001 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4070400.html
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