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Information card for entry 4070490
Preview
Coordinates | 4070490.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C46 H86 Au2 B2 F8 N2 P4 |
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Calculated formula | C46 H86 Au2 B2 F8 N2 P4 |
SMILES | [B](F)(F)(F)[F-].c12cccc(n2)C[P]([Au][P](Cc2cccc(n2)C[P]([Au][P](C1)(C(C)(C)C)C(C)(C)C)(C(C)(C)C)C(C)(C)C)(C(C)(C)C)C(C)(C)C)(C(C)(C)C)C(C)(C)C.[B](F)(F)(F)[F-] |
Title of publication | A Cationic AgI(PNPtBu) Species Acting as PNP Transfer Agent: Facile Synthesis of Pd(PNPtBu)(alkyl) Complexes and Their Reactivity Compared to PCPtBuAnalogues |
Authors of publication | van der Vlugt, Jarl Ivar; Siegler, Maxime A.; Janssen, Michèle; Vogt, Dieter; Spek, Anthony L. |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 24 |
Pages of publication | 7025 |
a | 13.723 ± 0.0004 Å |
b | 14.4624 ± 0.0006 Å |
c | 14.673 ± 0.0004 Å |
α | 90° |
β | 112.254 ± 0.002° |
γ | 90° |
Cell volume | 2695.2 ± 0.16 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0334 |
Residual factor for significantly intense reflections | 0.021 |
Weighted residual factors for significantly intense reflections | 0.0373 |
Weighted residual factors for all reflections included in the refinement | 0.0402 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.057 |
Diffraction radiation wavelength | 0.71073 Å |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4070490.html
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Users of the data should acknowledge the original authors of the
structural data.