Information card for entry 4070495

Structure parameters

• Formula: C55 H47 P3 Pd Si
• Calculated formula: C55 H47 P3 Pd Si
• Title of publication: Bis(o-phosphinophenyl)silane as a Scaffold for Dynamic Behavior of H−Si and C−Si Bonds with Palladium(0)
• Authors of publication: Takaya, Jun; Iwasawa, Nobuharu
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 23
• Pages of publication: 6636
• a: 16.617 ± 0.006 Å
• b: 10.69 ± 0.004 Å
• c: 25.34 ± 0.008 Å
• α: 90°
• β: 93.252 ± 0.012°
• γ: 90°
• Cell volume: 4494 ± 3 ų
• Cell temperature: 83 ± 2 K
• Ambient diffraction temperature: 83 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0447
• Residual factor for significantly intense reflections: 0.0326
• Weighted residual factors for significantly intense reflections: 0.0744
• Weighted residual factors for all reflections included in the refinement: 0.0816
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No