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Information card for entry 4070587
Preview
Coordinates | 4070587.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C66 H62 F6 N4 O8 P4 Rh2 S2 |
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Calculated formula | C66 H62 F6 N4 O8 P4 Rh2 S2 |
SMILES | [Rh]1([P](CC[P]1(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)(C#[O])=C1N(C=CN1C)CCN1C(=[Rh]2([P](CC[P]2(c2ccccc2)c2ccccc2)(c2ccccc2)c2ccccc2)C#[O])N(C=C1)C.S(=O)(=O)([O-])C(F)(F)F.S(=O)(=O)([O-])C(F)(F)F |
Title of publication | A-Frame Complexes of Dirhodium Bridged by Dicarbene and Diphosphine Ligands |
Authors of publication | Wells, Kyle D.; Ferguson, Michael J.; McDonald, Robert; Cowie, Martin |
Journal of publication | Organometallics |
Year of publication | 2008 |
Journal volume | 27 |
Journal issue | 4 |
Pages of publication | 691 |
a | 18.8274 ± 0.0017 Å |
b | 15.4094 ± 0.0014 Å |
c | 23.436 ± 0.002 Å |
α | 90° |
β | 98.2285 ± 0.0013° |
γ | 90° |
Cell volume | 6729.2 ± 1 Å3 |
Cell temperature | 193 ± 2 K |
Ambient diffraction temperature | 193 ± 2 K |
Number of distinct elements | 8 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0432 |
Residual factor for significantly intense reflections | 0.0336 |
Weighted residual factors for significantly intense reflections | 0.0899 |
Weighted residual factors for all reflections included in the refinement | 0.0996 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.047 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4070587.html
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Users of the data should acknowledge the original authors of the
structural data.