Information card for entry 4070602

Structure parameters

• Formula: C32 H35 B Cl5 N6 P Pt S3
• Calculated formula: C32 H35 B Cl5 N6 P Pt S3
• Title of publication: Retention of Pt→B Bonding in Oxidative Addition Reactions of the Platinaboratrane [Pt(PPh3){B(mt)3}](Pt→B)10(mt = Methimazolyl)
• Authors of publication: Crossley, Ian R.; Hill, Anthony F.; Willis, Anthony C.
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 3
• Pages of publication: 312
• a: 9.7438 ± 0.0002 Å
• b: 12.9979 ± 0.0002 Å
• c: 17.1896 ± 0.0003 Å
• α: 109.965 ± 0.0009°
• β: 101.305 ± 0.0013°
• γ: 93.5646 ± 0.0011°
• Cell volume: 1986.73 ± 0.06 ų
• Cell temperature: 200 K
• Ambient diffraction temperature: 200 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0374
• Residual factor for significantly intense reflections: 0.0261
• Weighted residual factors for all reflections: 0.0373
• Weighted residual factors for significantly intense reflections: 0.0276
• Weighted residual factors for all reflections included in the refinement: 0.0276
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1226
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No