Information card for entry 4070667

Structure parameters

• Formula: C62 H100 La2 N8 Si2
• Calculated formula: C62 H100 La2 N8 Si2
• SMILES: [La]123(N(C(C)(C)C)[Si]([N]51CC[N]2(C)CC[N]3(C)CC5)(C)C)(Cc1ccccc1)Cc1ccccc1.c1ccccc1
• Title of publication: Strategies for the Synthesis of Lanthanum Dialkyl Complexes with Monoanionic Ancillary Ligands
• Authors of publication: Bambirra, Sergio; Perazzolo, Francesca; Boot, Steven J.; Sciarone, Timo J. J.; Meetsma, Auke; Hessen, Bart
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 4
• Pages of publication: 704
• a: 17.277 ± 0.001 Å
• b: 9.771 ± 0.0006 Å
• c: 18.618 ± 0.001 Å
• α: 90°
• β: 94.561 ± 0.001°
• γ: 90°
• Cell volume: 3133 ± 0.3 ų
• Cell temperature: 100 ± 1 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 5
• Space group number: 7
• Hermann-Mauguin space group symbol: P 1 c 1
• Hall space group symbol: P -2yc
• Residual factor for all reflections: 0.0296
• Residual factor for significantly intense reflections: 0.0283
• Weighted residual factors for significantly intense reflections: 0.0643
• Weighted residual factors for all reflections included in the refinement: 0.065
• Goodness-of-fit parameter for all reflections included in the refinement: 0.972
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No